Scientific Production Faculty

Determination of oxytetracycline in milk samples by polymer inclusion membrane separation coupled to high performance liquid chromatography.



Páez Hernández, María Elena

2012

Pérez-Silva, I., Rodríguez J.A., Ramírez-Silva, M.T., Páez-Hernández, M.E. Determination of oxytetracycline in milk samples by polymer inclusion membrane separation coupled to high performance liquid chromatography, Analytica Chimica Acta, 2012, Vol. 718, p. 42-46, ISSN 0003-2670


Abstract


The determination of oxytetracycline in milk samples using a polymer inclusion membrane concept with high performance liquid chromatography (HPLC) was studied. The membranes developed are composed by cellulose acetate as polymer base, Cyanex 923 as carrier and o-nitrophenyl octyl ether as plasticizer. In the optimal conditions, the method exhibits good linearity in the range 0.030.20 mg L?1 with a limit of detection and quantification of 8.2 and 27.3 ?g L?1 respectively. The method was successfully applied to the analysis of milk samples with high selectivity.



Research Product




Related articles

Simultaneous determination of tetracyclines in poultry muscle by capillary zone electrophoresis

Multicommutated Anodic Stripping Voltammetry at Tubular Bismuth Film Electrode for Lead Determinatio...

Determination of non-steroidal anti-inflammatory drugs in wastewaters by magnetic matrix solid phase...

Study of the Humic Acid-Heavy Metal Interactions and Determination of their Stability Constants....

Electrochemical and AFM characterization of the electropolymerization of pyrrole over a graphiteepox...

Development of a novel composite sensor based on doped pyrrole selective to nitrate ions

Influence of the Cation Nature of the Sulphate Salt on the Electrochemical Synthesis of Sulfate-Dope...

Potentiometric Behavior of Diverse Polypyrrole-sulphate Films Electro Synthesized on Graphite - Epox...

Potentiometric quantification of saccharin by using a selective membrane formed by pyrrole electropo...

Validation of a tubular bismuth film amperometric detector: Determination of diclofenac sodium by mu...